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aqueous BOC Tert-butyloxy carbonyl d doublet DBU l,8-diazabicyclo[5.4.0]undec-7-ene DCE dichloroethane DCM dichloromethane DDQ 2,3 -Dichloro-5 ,6-dicyano- 1 ,4-benzoquinone DIPEA VA-diisopropylethylamine (Hiinig’s Base) DMAP 'A'-di meth l arm no pyridine DME 1 ,2-dimethoxyethane DMF dimethylformamide DMSO dimethylsulfoxide Dt doublet-triplet Eq equivalents ES/MS electrospray mass spectrometry Et ethyl EtOAc ethyl acetate EtOH ethanol (ethyl alcohol) FBS fetal bovine serum g grams HC1 hydrochloric acid hex hexanes HPLC/prep-HPLC high performance liquid chromatography /preparative HPLC h/Hr(s) hours Hz hertz IC50 half-maximal inhibitory concentration i-pr isopropyl J coupling constant (MHz) LC/MS Liquid chromatography/mass spectrometry LDA lithium diisopropylamide LHMDS Lithium bis(trimethylsilyl)amide M molar M multiplet M+ mass peak M+H+ mass peak plus hydrogen mCPBA meto-chloroperoxybenzoic acid Me methyl MeCN acetonitrile MeOH methanol (methyl alcohol) Mg milligram MgSCL magnesium sulfate MHz megahertz Min minute ml/mL milliliter mM millimolar mmol millimole NBS N-bromosuccinimide NaHCO 3 sodium bicarbonate n- normal NFSI N-fluorobenzenesulfonimide nM nanometer NMR nuclear magnetic resonance Pd/C Palladium on carbon Pd(OAc) 2 Palladium(II) acetate Ph phenyl PMB p-methoxybenzyl Q quartet q.s

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