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The delay between sample collection and analysis could lead to spuriously elevated acetone concentrations because of the spontaneous decarboxylation of acetoacetate (Van Stekelenburg & Koorevaar, 1972)
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Frequency:60
Samples were adjusted to pH 6.8–7.0, and 0.65 ml was transferred to a 5 mm NMR tube (Wilmad, Buena, NJ, USA)
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